• ornery_chemist@mander.xyz
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    2 months ago

    Like, so what if we store our tBuLi with other low-flash point flammables? And pyrophoric oxidizers? In the same bin? That’s stuck in a block of ice in the 30-year-old freezer because it hasn’t ever been de-iced?

    What if the power goes out for a long period of time and the tBuLi goes for a swim? Or we say you have to de-ice the freezer?

    Haha sounds crazy. And, I wouldn’t have to do the shitty quench before disposal. Or work on that project anymore.

    Because you’re injured or because PI fires you?

    Haha, yeah :)

    :|

    :)

    :|

    Oh, while you’re here, does this still smell like DCM? I can’t tell if I rotavapped it all off and the NMR tubes all need aqua regia (sorry my b).

    • TonyTonyChopper@mander.xyz
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      2 months ago

      Aqua regia isn’t even that scary. Try pipetting pure bromine while it shoots itself out from constantly evaporating

      • ornery_chemist@mander.xyz
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        6 days ago

        Aqua regia ain’t no piranha, and also ain’t the most concerning thing in my post lol.

        Ah bromine. Super dense, low MW, and low bp, all making dosing accurate amounts a heroic feat. If you store your bromine cold, you can precool the pipette by sucking up and spitting out a few times before transfering, which helps cut down the vapor.